Magnetic suspension balance. Gravimetric sorption in real-world conditions. Dual-sample testing, up to 400°C.
● Various single-photon-counting X-ray detectors.
● Pure Kα1 radiation using Co, Cu, Mo and Ag sources.
● Transmission/Debye-Scherrer or Bragg-Brentano mode.
Introduction
The well-known, high-precision STOE STADI P two circle goniometer is the basis of STOE’s powder diffraction building block system (read more about it here). Vertically or horizontally mounted, the STADI P can be built in Transmission/Debye-Scherrer or Bragg-Brentano geometry. Moreover, two STADI P goniometers, either in the same or different configurations, can be mounted in the same cabinet resulting in two completely independent instruments. However, the two goniometers can also share one source.
Specifications
| 2θ range | 0° up to 140° 2θ |
|---|---|
| Goniometer | 2 circles |
| Radius of measuring circle | 260 mm |
| Radius of focusing circle | 130 mm |
| X-ray sources | Sealed Tubes: Co, Cu, Mo, Ag |
| Optics | Primary monochromator |
| Software | WinXPOW package |
| Dimensions (including system cabinet, max.) | 1800 x 880 x 2050 mm |
| Weight (complete system) | 780 – 940 kg |
| Detectors | Silicon strip detector MYTHEN2 R 1K/2K/3K/4K |
| Accessories |
|
ADAMAnT
When an X-ray tube ages, it is possible that its take off angle changes, resulting in a 2 Theta shift of the reflex positions on the detector. To reverse the impact of this take off angle change, the monochromator and sample position have to be adapted through a Beam Optimization.
The STOE STADI P Beam Optimization has been a well-established tool of the WinXPOW software for a very long time. It automatically sets the Johann type monochromator to the maximum intensity of the Kα1-radiation of a sealed tube’s line focus by the help of a certified standard material – but the alignment of the goniometer axis into the beam path has – so far – still to be done manually with a luminance screen.
From now on, the unique ADAMAnT tool aligns monochromator and goniometer automated to the Kα1-radiation, making any contact with the open beam or its air scattered radiation no longer necessary, no matter whether it is only the exchange of a worn-out tube by a new one with the same anode material or whether the radiation should be swapped to a different one.
The ADAMAnT is available for all typical anode materials (Co, Cu, Mo, Ag) but currently only for horizontal setups, with plans for future availability in vertical configurations and conveniently, can be integrated into existing horizontal STADI P diffractometers.
STADi P for pdf data collection
As the demand for materials with lower degrees of order continues to rise, the significance of Pair Distribution Function (PDF) measurements is growing steadily. To measure best possible data for PDF interpretation, the STADI P can be installed with Ag Kα1 radiation and expanded with a PDF collimator, a MYTHEN2 4K detector and optionally air scattering shields, without any loss in diffraction data quality.
Software & Accessories
WinXPOW, is a uniquely designed powder diffraction software developed exclusively by our skilled team at STOE. It is meticulously crafted to perfectly work with our instruments, ensuring seamless compatibility and optimal performance. In addition to controlling the instruments, WinXPOW provides a comprehensive range of cutting-edge features. These include data reduction, profile fitting, pattern indexing, and spacegroup determination. Moreover, it boasts an array of powerful functionalities, such as advanced 2D and 3D graphics, among numerous other capabilities.
We provide a wide range of accessories to customize your sample environment according to your specific requirements. Our products encompass high temperature and reaction chambers, sample changers, dedicated battery cell holders, and various other accessories to enhance your experimentation capabilities.
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